1,3,5-三溴-1,3,5-噻嗪烷-2,4,6-三酮合成路线 (共 10 条)
反应条件
sodium hydroxide; Oxonereg;; sodium carbonate; potassium bromide T=20°C; 24 h;
参考文献
De Almeida, Leonardo S.; Esteves, Pierre M.; De Mattos, Marcio C. S.
Synlett, 2006 , # 10 p. 1515 - 1518
反应条件
in aceton/CCL4 suspn. under N2, 130-170°C; sublimated 230-250°C, 1 Torr;
参考文献
Gotthardi
Monatshefte fuer Chemie, 1967 , vol. 98, # 4 p. 1613
Full Text View citing articles Show Details
Gmelin Handbook: C: MVol.D3, 5.6.2, page 147 - 147
参考文献
Gottardi
Angewandte Chemie, 1971 , vol. 83, p. 445
Full Text Show Details
Gottardi, W.
Angewandte Chemie, International Edition in English, 1971 , vol. 10, p. 416
Full Text Show Details
Gottardi, W.
Monatshefte fuer Chemie, 1972 , vol. 103, p. 1150 - 1157
Full Text View citing articles Show Details
Gmelin Handbook: C: MVol.D3, 5.3, page 142 - 143
反应条件
bei mehrtaegiger Einw. von Sonnenlicht;
参考文献
Birckenbach; Linhard
Chemische Berichte, 1929 , vol. 62, p. 2263,2273
反应条件
in absence of water, 120-150°C, 14d;
参考文献
Gottardi, W.
Monatshefte fuer Chemie, 1972 , vol. 103, p. 1150 - 1157
Full Text View citing articles Show Details
Gmelin Handbook: C: MVol.D3, 5.6.2, page 147 - 147
参考文献
Gotthardi
Monatshefte fuer Chemie, 1967 , vol. 98, # 4 p. 1613
Full Text View citing articles Show Details
Gmelin Handbook: C: MVol.D3, 5.6.2, page 147 - 147
参考文献
Gotthardi
Monatshefte fuer Chemie, 1967 , vol. 98, # 4 p. 1613
Full Text View citing articles Show Details
Gmelin Handbook: C: MVol.D3, 5.6.2, page 147 - 147
反应条件
depolymn. of 99.6percent (BrNCO)3, 300°C, 1 Torr, 48h; impurity: bromine, isocynic acid, carbonylisocyanante;
参考文献
Gerke, M.; Schatte, G.; Willner, H.
Journal of Molecular Spectroscopy, 1989 , vol. 135, p. 359 - 369
反应条件
sodium hydroxide in diethyl ether; water T=20°C; 24 h; Green chemistry; Mechanism; regioselective reaction;
参考文献
Sodre, Leonardo R.; Esteves, Pierre M.; De Mattos, Marcio C. S.
Journal of the Brazilian Chemical Society, 2013 , vol. 24, # 2 p. 212 - 218
反应条件
sodium hydroxide in diethyl ether; water
T=20°C; 24 h; Green chemistry; Mechanism; regioselective reaction;
参考文献
Sodre, Leonardo R.; Esteves, Pierre M.; De Mattos, Marcio C. S.
Journal of the Brazilian Chemical Society, 2013 , vol. 24, # 2 p. 212 - 218