4-甲基-1,2-噁唑-3-胺合成路线 （共 4 条）
反应条件
1: methyl acrylonitrile With bromine in methanol T=0 - 35°C; 2 h; 2: amino-hydroxamic acid With sodium hydroxide in methanol; water T=0°C; 2.5 h; Heating / reflux;
参考文献
WO2007/99326 A1, ;
Page/Page column 123-124 ;
WO 2007/099326 A1
反应条件
1: With bromine in methanol T=0 - 35°C; 2 h; 2: With sodium hydroxide; amino-hydroxamic acid in methanol; water T=0°C; 2.5 h; Heating / reflux;
参考文献
US2009/76075 A1, ;
Page/Page column 43 ;
反应条件
1: methyl acrylonitrile With bromine in methanol T=0 - 35°C; 2 h; 2: amino-hydroxamic acid With sodium hydroxide in methanol; water T=0°C; 2.5 h; Heating / reflux;
参考文献
WO2007/113565 A1, ;
Page/Page column 106 ;
WO 2007/113565 A1
反应条件
sodium hydroxide; amino-hydroxamic acid in methanol
参考文献
Monatshefte fuer Chemie, , vol. 101, p. 1109 - 1122
