2,2-二甲基-3-氧代-3-苯丙醛合成路线 （共 12 条）
反应条件
(i) Et2O, (ii) aq. HCl; Multistep reaction;
参考文献
Adam, Waldemar; Maas, Wiebke
Journal of Organic Chemistry, 2000 , vol. 65, # 22 p. 7650 - 7655
反应条件
1: With oxalyl dichloride in dichloromethane T=38°C; Vilsmeier-Haack reaction; 24 h; Inert atmosphere; 2: With sodium hydrogencarbonate in dichloromethane; water Inert atmosphere;
参考文献
Hassan, Jamal; Richards, Christopher J.
Synlett, 2012 , # 2 p. 239 - 242
反应条件
1: 2: With water Further stages.;
参考文献
Bezzenine-Lafollee, Sophie; Guibe, Francois; Villar, Helene; Zriba, Riadh
Tetrahedron, 2004 , vol. 60, # 32 p. 6931 - 6944
反应条件
1: diethyl ether 2: diethyl ether / Ambient temperature View Scheme
参考文献
Armesto, Diego; Ramos, Ana; Perez-Ossorio, Rafael
Tetrahedron Letters, 1982 , vol. 23, # 49 p. 5195 - 5198
反应条件
2-(dimethylamino)-ethanol in hexane; toluene 56 h;
参考文献
Soai, Kenso; Watanabe, Masami; Koyano, Masashi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 6 p. 2124 - 2125
反应条件
sodium acetate; acetic acid in tert-butyl alcohol 16 h; Heating;
参考文献
Lee, Sze-Ming; Sammes, Michael P.
Journal of Chemical Research, Miniprint, 1990 , # 10 p. 2401 - 2410
反应条件
sodium acetate; acetic acid in tert-butyl alcohol 16 h; Heating;
参考文献
Lee, Sze-Ming; Sammes, Michael P.
Journal of Chemical Research, Miniprint, 1990 , # 10 p. 2401 - 2410
反应条件
Bu4N(OAc)3BH T=75 - 80°C; 24 h; Mechanism;
参考文献
Nutaitis, Charles F.; Gribble, Gordon W.
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4287 - 4290
反应条件
1: diethyl ether 2: 100 percent / water / diethyl ether / Ambient temperature View Scheme
参考文献
Armesto, Diego; Ramos, Ana; Perez-Ossorio, Rafael
Tetrahedron Letters, 1982 , vol. 23, # 49 p. 5195 - 5198
反应条件
sodium acetate; acetic acid in tert-butyl alcohol 16 h; Heating;
参考文献
Lee, Sze-Ming; Sammes, Michael P.
Journal of Chemical Research, Miniprint, 1990 , # 10 p. 2401 - 2410
