2,3-喹啉二甲酸二甲酯合成路线 (共 14 条)
反应条件
trichlorophosphate in N-methyl-acetamide; 1,2-dichloro-ethane
反应条件
indium(III) chloride; SnCl2·2H2O in ethanol 3.5 h; Reflux; regioselective reaction;
参考文献
Chanda, Tanmoy; Verma, Rajiv Kumar; Singh, Maya Shankar
Chemistry - An Asian Journal, 2012 , vol. 7, # 4 p. 778 - 787
反应条件
phosphorus trichoride in chloroform 8 h; Heating;
参考文献
Rozhkov; Piskunova; Gol'd; Kalvin'sh
Chemistry of Heterocyclic Compounds, 1998 , vol. 34, # 1 p. 77 - 91
反应条件
indium(III) chloride in acetonitrile 10 h; Reflux; regioselective reaction;
参考文献
Chanda, Tanmoy; Verma, Rajiv Kumar; Singh, Maya Shankar
Chemistry - An Asian Journal, 2012 , vol. 7, # 4 p. 778 - 787
反应条件
triethylamine in benzene T=70°C; 24 h;
参考文献
Heterocycles, , vol. 41, # 8 p. 1675 - 1682
反应条件
1: 61.5 percent / sodium, methanol / 0 - 5 °C 2: 88 percent / phosphorus trichloride / CHCl3 / 8 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 34, # 1 p. 77 - 91
反应条件
1: 61.5 percent / sodium, methanol / 0 - 5 °C 2: 88 percent / phosphorus trichloride / CHCl3 / 8 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 34, # 1 p. 77 - 91
反应条件
sulfuric acid 1.) MeOH, reflux; 2.) MeOH, CHCl3, reflux; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 35, # 21 p. 3613 - 3616
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 116, p. 51
反应条件
T=90°C; 240 h; other 2,1-benzisothiazoles, other dienophiles; var. temp. and reaction time; Mechanism;
参考文献
Bryce, Martin R.; Acheson, R. Morrin; Rees, Anthony J.
Heterocycles, 1983 , vol. 20, # 3 p. 489 - 495