(1-叔丁基乙烯氧基)三甲基硅烷合成路线 （共 67 条）
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride 1.) CH2Cl2, room temperature, 10 h, 2.) DMF, room temperature, 24 h; Yield given. Multistep reaction;
参考文献
Matano, Yoshihiro; Azuma, Nagao; Suzuki, Hitomi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1739 - 1748
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride; potassium bromide 1.) CH2Cl2, room temperature, 10 h, 2.) DMF, room temperature, 24 h; Yield given. Multistep reaction;
参考文献
Yoshikawa, Takashi; Mori, Seiji; Shindo, Mitsuru
Tetrahedron, 2009 , vol. 65, # 43 p. 8832 - 8838
反应条件
(CF3CH2O)VOCl2 T=-78°C; 0.5 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
chloromethyl iodide 1.) 3 h, 2.) DMSO, RT, 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Miyano, Sotaro; Hokari, Hiroshi; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 534 - 539
反应条件
boron trifluoride diethyl etherate in dichloromethane
参考文献
Yoshimatsu, Mitsuhiro; Naito, Motoyo; Shimizu, Hiroshi; Muraoka, Osamu; Tanabe, Genzoh; Kataoka, Tadashi
Journal of Organic Chemistry, 1996 , vol. 61, # 23 p. 8200 - 8206
反应条件
BnNMe3(+)F(-) in tetrahydrofuran T=20°C; 16 h; further reagent: CsF, Bu4NF, KH;
参考文献
Hirsch, Elisabeth; Huenig, Siegfried; Reissig, Hans-Ulrich
Chemische Berichte, 1982 , vol. 115, # 12 p. 3687 - 3696
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Hirsch, Elisabeth; Huenig, Siegfried; Reissig, Hans-Ulrich
Chemische Berichte, 1982 , vol. 115, # 12 p. 3687 - 3696
反应条件
XeF2 in acetonitrile T=20°C; 1 h;
参考文献
Organic Letters, , vol. 1, # 10 p. 1591 - 1594
反应条件
4-tolylthallium(III) bis(trifluoroacetate); titanium tetrachloride 1.) benzene, RT, 30 min, 2.) THF, -78 deg C, 1.5 h, RT, 1 h; Yield given. Multistep reaction;
参考文献
Moriarty, Robert M.; Penmasta, Raju; Prakash, Indra; Awasthi, Alok K.
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 1022 - 1025
反应条件
1: With titanium tetrachloride in dichloromethane T=-78 - -50°C; Mukaiyama reaction; 2: With ammonium chloride T=-50 - 0°C; Title compound not separated from byproducts;
参考文献
Lalic, Gojko; Petrovski, Zeljko; Galonic, Danica; Matovic, Radomir; Saicic, Radomir N
Tetrahedron, 2001 , vol. 57, # 3 p. 583 - 591
