(1-叔丁基乙烯氧基)三甲基硅烷合成路线 （共 67 条）
反应条件
trimethylsilyl trifluoromethanesulfonate; [VO(OEt)Cl2] in dichloromethane T=-75°C; Yield given. Yields of byproduct given;
参考文献
Hirao, Toshikazu; Fujii, Takashi; Ohshiro, Yoshiki
Tetrahedron, 1994 , vol. 50, # 34 p. 10207 - 10214
反应条件
(CF3CH2O)VOCl2 T=-78°C; 0.5 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
lithium perchlorate in nitromethane 16 h; Ambient temperature; Yields of byproduct given;
参考文献
Chini, Marco; Crotti, Paolo; Gardelli, Cristina; Minutolo, Filippo; Pineschi, Mauro
Gazzetta Chimica Italiana, 1993 , vol. 123, # 12 p. 673 - 676
反应条件
lithium perchlorate 16 h; Ambient temperature; Yields of byproduct given;
参考文献
Chini, Marco; Crotti, Paolo; Gardelli, Cristina; Minutolo, Filippo; Pineschi, Mauro
Gazzetta Chimica Italiana, 1993 , vol. 123, # 12 p. 673 - 676
反应条件
copper dichloride in N,N-dimethyl-formamide 1) r.t., 3 h, 2) 50 deg C, 30 min; further reagent: FeCl3 in MeCN;
参考文献
Ito, Yoshihiko; Nakatsuka, Masashi; Saegusa, Takeo
Journal of Organic Chemistry, 1980 , vol. 45, p. 2022 - 2024
反应条件
(i) 9-borabicyclo-(3,3,1)-nonane, (ii) aq. H2O2, NaOH; Multistep reaction;
参考文献
Larson,G.L.; Fuentes,L.M.
Synthetic Communications, 1979 , vol. 9, p. 841 - 844
反应条件
1: FeCl3 2: H2 / Raney-Ni View Scheme
参考文献
Reetz,M.T. et al.
Tetrahedron Letters, 1979 , p. 4971 - 4974
反应条件
(CF3CH2O)VOCl2 T=-78°C; 0.5 h;
参考文献
Ryter; Livinghouse
Journal of the American Chemical Society, 1998 , vol. 120, # 11 p. 2658 - 2659
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
1: With P(N(CH2Ph)CH2CH2)3N in tetrahydrofuran T=0°C; Mukaiyama reaction; 72 h; Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran T=0°C; 12 h; Inert atmosphere;
参考文献
Chintareddy, Venkat Reddy; Wadhwa, Kuldeep; Verkade, John G.
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8118 - 8132
