(1-叔丁基乙烯氧基)三甲基硅烷合成路线 (共 67 条)
反应条件
in chloroform
T=20 - 25°C; 1.5 h;
参考文献
Anders, Ernst; Stankowiak, Achim; Riemer, Roland
Synthesis, 1987 , # 10 p. 931 - 934
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
Ambient temperature;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
in dichloromethane
T=90°C; 20 h;
参考文献
Gostevskii; Voronkov; Rakhlin; Mirskov
Russian Journal of General Chemistry, 2005 , vol. 75, # 5 p. 827 - 828
反应条件
in benzene-d6
HSiMe3 added by vacuum transfer, heated to 85°C for 2 h; not isolated; NMR;
参考文献
Hartwig, John F.; Bergman, Robert G.; Andersen, Richard A.
Organometallics, 1991 , vol. 10, p. 3344 - 3362
反应条件
N,N,N',N,-tetramethylethylenediamine in pentane
参考文献
West,R.; Gornowicz,G.A.
Journal of Organometallic Chemistry, 1971 , vol. 28, p. 25 - 35
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Gerval,P.; Frainnet,E.
Journal of Organometallic Chemistry, 1978 , vol. 153, p. 137 - 151
反应条件
in benzene
0.5 h; Ambient temperature;
参考文献
Shipov, A. G.; Kramarova, E. P.; Artamkina, O. B.; Oleneva, G. I.; Nepomnyashchaya, N. A.; Baukov, Yu. I.
Russian Journal of General Chemistry, 1995 , vol. 65, # 2.2 p. 233 - 240
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 2 p. 272 - 280
反应条件
1: 63 percent / triethylamine / benzene / 24 h / Ambient temperature
2: 44 percent / benzene / 0.5 h / Ambient temperature
View Scheme
参考文献
Shipov, A. G.; Kramarova, E. P.; Artamkina, O. B.; Oleneva, G. I.; Nepomnyashchaya, N. A.; Baukov, Yu. I.
Russian Journal of General Chemistry, 1995 , vol. 65, # 2.2 p. 233 - 240
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 2 p. 272 - 280
反应条件
potassium cyanide; 18-crown-6 ether in diethyl ether
参考文献
Kruglaya,O.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1979 , vol. 49, # 2 p. 354 - 360,308 - 313
反应条件
1,1,1,3,3,3-hexamethyl-disilazane
参考文献
Miller,R.D.; McKean,D.R.
Synthesis, 1979 , p. 730 - 732