(1-叔丁基乙烯氧基)三甲基硅烷合成路线 （共 67 条）
参考文献
Cazeau,P. et al.
Journal of Organometallic Chemistry, 1976 , vol. 105, p. 145 - 156
反应条件
trimethylsilyl trifluoromethanesulfonate in chloroform
T=0°C; Sakurai-Hosomi reaction; 1 h;
参考文献
Kobashi, Yohei; Minowa, Tomofumi; Mukaiyama, Teruaki
Chemistry Letters, 2005 , vol. 34, # 6 p. 756 - 757
反应条件
1: 1.) TiCl4, Ti(i-PrO)4 / 1.) dichloromethane, -78 deg C, 30 min, 2.) dichloromethane, -50 deg C, 18 h
2: 74 percent / sodium hydride / tetrahydrofuran; hexamethylphosphoric acid triamide / 2 h / Heating
View Scheme
参考文献
Wada, Eiji; Funakoshi, Junji; Kanemasa, Shuji
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 9 p. 2456 - 2464
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-78°C; parallel recognition; 5 h;
参考文献
Chen, Jian-Xie; Sakamoto, Katsumasa; Orita, Akihiro; Otera, Junzo
Tetrahedron, 1998 , vol. 54, # 29 p. 8411 - 8420
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride
1.) CH2Cl2, room temperature, 10 h, 2.) THF, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Matano, Yoshihiro; Azuma, Nagao; Suzuki, Hitomi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1739 - 1748
反应条件
1: ethylene oxide / -15 °C / Irradiation
2: DBN / CH2Cl2 / -78 °C
View Scheme
参考文献
Hayashi, Masaji; Mukaiyama, Teruaki
Chemistry Letters, 1987 , p. 1283 - 1286
反应条件
in 1,2-dichloro-ethane
T=25°C; 2.5 h;
参考文献
Hofmann, Karin; Simchen, Gerhard
Liebigs Annalen der Chemie, 1984 , # 1 p. 39 - 47
反应条件
bis (triortho-tolylphosphine)palladium(II) chloride; tri-n-butyltin fluoride in benzene
24 h; Heating;
参考文献
Kuwajima, Isao; Urabe, Hirokazu
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6831 - 6833
反应条件
Diphenyliodonium fluoride in tetrahydrofuran
1) 37 min, -40 deg C 2) 1.8 h, to 6 deg C 3) 5.5 h, r.t.;
参考文献
Chen, Kuanchiang; Koser, Gerald F.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5764 - 5767
反应条件
pyridine
T=0°C; 2 h;
参考文献
Sakakura, Toshiyasu; Hara, Masayasu; Tanaka, Masato
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 3 p. 283 - 288
