(1-叔丁基乙烯氧基)三甲基硅烷合成路线 （共 67 条）
反应条件
in tetrahydrofuran
1) 37 min, -40 deg C 2) 1.8 h, to 6 deg C 3) 5.5 h, r.t.;
参考文献
Chen, Kuanchiang; Koser, Gerald F.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5764 - 5767
反应条件
1: With P(N(CH2Ph)CH2CH2)3N in tetrahydrofuran
T=0°C; Mukaiyama reaction; 72 h; Inert atmosphere;
2: With hydrogenchloride; water in tetrahydrofuran
T=0°C; 12 h; Inert atmosphere;
参考文献
Chintareddy, Venkat Reddy; Wadhwa, Kuldeep; Verkade, John G.
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8118 - 8132
反应条件
zinc(II) iodide in diethyl ether
T=22°C; 2 h;
参考文献
Reetz, Manfred T.; Mueller-Starke, H.
Liebigs Annalen der Chemie, 1983 , # 10 p. 1726 - 1738
反应条件
zinc(II) chloride in dichloromethane
T=-25°C; 4 h;
参考文献
Reetz, Manfred T.; Mueller-Starke, H.
Liebigs Annalen der Chemie, 1983 , # 10 p. 1726 - 1738
反应条件
zinc(II) chloride in dichloromethane
T=22°C; 2 h;
参考文献
Reetz, Manfred T.; Mueller-Starke, H.
Liebigs Annalen der Chemie, 1983 , # 10 p. 1726 - 1738
反应条件
zinc dibromide in dichloromethane
T=20°C; 3 h;
参考文献
Alexander, Rikki P.; Paterson, Ian
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5911 - 5914
反应条件
zinc dibromide in dichloromethane
T=20°C; 3 h;
参考文献
Alexander, Rikki P.; Paterson, Ian
Tetrahedron Letters, 1983 , vol. 24, # 52 p. 5911 - 5914
反应条件
in benzene
T=10 - 15°C; 4 h; Irradiation; Yields of byproduct given;
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
反应条件
in benzene
T=10 - 15°C; 4 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
反应条件
1: 86 percent / benzene / 4 h / 10 - 15 °C / Irradiation
2: 51 percent / p-toluenesulfonic acid / CCl4; methanol / 24 h / Ambient temperature
View Scheme
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
