2-甲基-5-三氟甲基呋喃合成路线 (共 5 条)
反应条件
copper(I) sulfate in quinoline T=230°C;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1362846 A1, 2003 ;
Location in patent: Page/Page column 125 ;
EP 1362846 A1
反应条件
toluene-4-sulfonic acid in toluene 55 h; Heating;
参考文献
Smith, Jonathan O.; Mandal, Braja K.; Filler, Robert; Beery, James W.
Journal of Fluorine Chemistry, 1997 , vol. 81, # 2 p. 123 - 128
反应条件
[bis(acetoxy)iodo]benzene; silver fluoride in dimethyl sulfoxide T=20°C; 20 h;
参考文献
Chemical Communications, , vol. 49, # 57 p. 6385 - 6387
反应条件
1: 73 percent / aq. NaCl / dimethylsulfoxide / 2.5 h / 110 °C 2: 42 percent / p-TsOH / toluene / 55 h / Heating View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 81, # 2 p. 123 - 128
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in chloroform 0.25 h; Heating / reflux;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1362846 A1, 2003 ;
Location in patent: Page/Page column 125 ;
EP 1362846 A1