反应条件
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.83 h / 0 - 20 °C 2.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 0.17 h / 150 °C / |Microwave irradiation 3.1: trimethylaluminum / toluene; dichloromethane / 1.08 h / -10 - 20 °C / |Inert atmosphere 3.2: 20 °C / |Reflux 3.3: 0.5 h View Scheme
参考文献
Weinstock, Joseph; Wu, Jian; Cao, Ping; Kingsbury, William D.; McDermott, Jeffrey L.; Kodrasov, Matthew P.; McKelvey, Devin M.; Suresh Kumar, K. G.; Goldenberg, Seth J.; Mattern, Michael R.; Nicholson, Benjamin
Medicinal Chemistry letters, 2012 , vol. 3, # 10 p. 789 - 792,4
Title/Abstract Full Text Show Details
Weinstock, Joseph; Wu, Jian; Cao, Ping; Kingsbury, William D.; McDermott, Jeffrey L.; Kodrasov, Matthew P.; McKelvey, Devin M.; Suresh Kumar; Goldenberg, Seth J.; Mattern, Michael R.; Nicholson, Benjamin
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 10 p. 789 - 792