3-氯-5,5-二甲基-2-环己烯-1-酮合成路线 (共 38 条)
参考文献
Crossley; Le Sueur
Journal of the Chemical Society, 1903 , vol. 83, p. 116,128
反应条件
in diethyl ether 96 h; Ambient temperature;
参考文献
Gompper, Rudolf; Kottmair, Eduard
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 6 p. 833 - 847
参考文献
Davis,B.R.; Woodgate,P.D.
Journal of the Chemical Society, 1965 , p. 5943 - 5948
反应条件
in diethyl ether T=0°C; 1 h;
参考文献
Piers, Edward; Cheng, Kin Fai; Nagakura, Isao
Canadian Journal of Chemistry, 1982 , vol. 60, p. 1256 - 1263
参考文献
Alt,G.H.; Speziale,A.J.
Journal of Organic Chemistry, 1964 , vol. 29, p. 794 - 797
反应条件
1: H2 / 5percent palladium on charcoal 2: 1.) PCl5, 2.) NaOEt / 2.) reflux, 19 h 3: 69 percent / Na 4: 50 percent / AlCl3 / CH2Cl2 / 6.25 h / 0 °C 5: H2 / 5percent Pd-C / ethanol View Scheme
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
反应条件
1: Kochen des Reaktionsproduktes mit alkoh. Schwefelsaeure
2: concentrated hydrochloric acid
View Scheme
参考文献
Crossley; Gilling
Journal of the Chemical Society, 1910 , vol. 97, p. 528
反应条件
Yield given. Multistep reaction;
参考文献
Comasseto, Joao V.; Lo, Wai L.; Petragnani, Nicola
Tetrahedron, 1997 , vol. 53, # 22 p. 7445 - 7460
反应条件
in methanol
18 h; Ambient temperature;
参考文献
Nelson
Synthesis, 1992 , # 12 p. 1287 - 1290
反应条件
potassium iodide; zinc in methanol
1 h; Heating / reflux;
参考文献
SERENEX, INC.
Patent: US2008/119457 A1, 2008 ;
Location in patent: Page/Page column 50 ;