乙酰苯-β,β,β-d3合成路线 (共 19 条)
反应条件
4 A molecular sieve; water-d2 T=180°C; P=9000.72 Torr; 0.5 h; microwave irradiation;
参考文献
Yamamoto, Mitsuru; Oshima, Koichiro; Matsubara, Seijiro
Chemistry Letters, 2004 , vol. 33, # 7 p. 846 - 847
反应条件
1: With triphenylphosphine in tetrahydrofuran T=50°C; 36 h; 2: With potassium cyanide; water-d2 in tetrahydrofuran T=50 - 60°C; 48 h;
参考文献
Lee, Ka Young; Na, Jeong Eun; Lee, Mi Jung; Kim, Jae Nyoung
Tetrahedron Letters, 2004 , vol. 45, # 31 p. 5977 - 5981
反应条件
hydrogenchloride; water-d2; N-hexadecyl-N,N,N-trimethylammonium bromide in isopropyl alcohol T=140°C; 7 h;
参考文献
Nairoukh, Zackaria; Avnir, David; Blum, Jochanan
ChemSusChem, 2013 , vol. 6, # 3 p. 430 - 432
反应条件
aluminium trichloride 1 h; Ambient temperature;
参考文献
Neubert, Mary E.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 129, p. 327 - 374
反应条件
water-d2; sodium 72 h; Heating; Title compound not separated from byproducts;
参考文献
Bapat, Jayant B.; Brown, Roger F.C.; Bulmer, Glenn H.; Childs, Trevor; Coulston, Karen J.; Eastwood, Frank W.; Taylor, Dennis K.
Australian Journal of Chemistry, 1997 , vol. 50, # 12 p. 1159 - 1182
反应条件
NaOD; water-d2 72 h; Reflux;
参考文献
Riches, Samantha L.; Saha, Chandreyee; Filgueira, Noelia Fontan; Grange, Emma; McGarrigle, Eoghan M.; Aggarwal, Varinder K.
Journal of the American Chemical Society, 2010 , vol. 132, # 22 p. 7626 - 7630
参考文献
Baumstark, Alfons L.; Vasquez, Pedro C.; Cunningham, Mark; Leggett-Robinson, Pamela M.
Heterocyclic Communications, 2010 , vol. 16, # 4-6 p. 217 - 220
反应条件
potassium deuteroxide; water-d2 T=25°C; Rate constant;
参考文献
Alston II, William C.; Haley, Kari; Kanski, Ryszard; Murray, Christopher J.; Pranata, Julianto
Journal of the American Chemical Society, 1996 , vol. 118, # 28 p. 6562 - 6569
反应条件
3,3-dimethyldioxirane in acetone T=0°C; Kinetics;
参考文献
Angelis, Yiannis S.; Hatzakis, Nikos S.; Smonou, Ioulia; Orfanopoulos, Michael
Tetrahedron Letters, 2001 , vol. 42, # 22 p. 3753 - 3756
反应条件
2: chromic acid View Scheme
参考文献
Balzer, Hartmut H.; Berger, Stefan
Magnetic Resonance in Chemistry, 1990 , vol. 28, # 5 p. 437 - 442