3-氨基-5-羟基-1-戊烯合成路线 (共 3 条)
反应条件
water; trifluoroacetic acid in dichloromethane T=20°C; 1 h;
参考文献
Ragains, Justin R.; Winkler, Jeffrey D.
Organic Letters, 2006 , vol. 8, # 20 p. 4437 - 4440
反应条件
n-butyllithium in tetrahydrofuran; hexane T=20°C; Wittig reaction; 6.5 h;
参考文献
Zhang, Zongren; Ding, Yu-Shin; Studenov, Andrei R.; Gerasimov, Madina R.; Ferrieri, Richard A.
Journal of Labelled Compounds and Radiopharmaceuticals, 2002 , vol. 45, # 3 p. 199 - 211
反应条件
1: 72 percent / diisobutylaluminum hydride / toluene; CH2Cl2 / 6.5 h / -72 °C 2: 4 percent / BuLi / tetrahydrofuran; hexane / 6.5 h / 20 °C View Scheme
参考文献
Ding, Y.-S.; Studenov, A. R.; Zhang, Z.; Gerasimov, M.; Schiffer, W.; Dewey, S. L.; Telang, F.
Journal of Labelled Compounds and Radiopharmaceuticals, 2001 , vol. 44, p. S1008 - S1010