反应条件
1.1: acetic anhydride / acetic acid / 0.33 h / 110 °C
1.2: 30 h / 110 °C
1.3: 1 h / 70 °C
2.1: methanol; potassium carbonate / 20 h / 20 °C
3.1: PCC-alumina / hexane / 20 °C
4.1: copper(l) iodide / tetrahydrofuran; hexane / 0.25 h / -5 °C
4.2: 2 h / -78 °C
5.1: ethylaluminum dichloride / hexane; 1,2-dichloro-ethane / 1.5 h / 55 °C
View Scheme
参考文献
Demuynck, Anneleen L. W.; Levecque, Pieter; Kidane, Aklilu; Gammon, David W.; Sickle, Eugene; Jacobs, Pierre A.; De Vos, Dirk E.; Sels, Bert F.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3419 - 3430
