三甲基-[4-(三甲基硅烷基甲基)苄基]硅烷合成路线 (共 9 条)
反应条件
lithium in tetrahydrofuran T=0°C; 1 h;
参考文献
Gomez, Cecilia; Huerta, Fernando F.; Yus, Miguel
Tetrahedron, 1997 , vol. 53, # 40 p. 13897 - 13904
反应条件
1: n-butyllithium, potassium tert-butoxide / hexane / 1 h / Heating 2: pentane View Scheme
参考文献
Bates, Robert B.; Hess, B. Andes; Ogle, Craig A.; Schaad, L.J.
Journal of the American Chemical Society, 1981 , vol. 103, # 17 p. 5052 - 5058
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether 15 h; Ambient temperature;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Okamoto, Yasuo; Kumada, Makoto
Tetrahedron Letters, 1981 , vol. 22, # 44 p. 4449 - 4452
参考文献
Gallagher, Michael J.; Harvey, Stephen; Raston, Colin L.; Sue, Rodney E.
Journal of the Chemical Society, Chemical Communications, 1988 , # 4 p. 289 - 290
反应条件
potassium in tetrahydrofuran Heating;
参考文献
Bock,H.; Kaim,W.
Chemische Berichte, 1978 , vol. 111, p. 3552 - 3572
参考文献
Tamao,K. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 1958 - 1969
反应条件
n-butyllithium; potassium 2-methyl-2-butoxide 1) hexane, 16 h, r.t.; 6 h, reflux, 2) hexane, -78 deg C; r.t., 20 h; Yield given. Multistep reaction;
参考文献
Wilhelm, Dieter; Clark, Timothy; Friedl, Thomas; Schleyer, Paul von Rague
Chemische Berichte, 1983 , vol. 116, # 2 p. 751 - 760
反应条件
n-butyllithium; pmdien in hexane Ambient temperaturelithiation of p-xylene compounds, comparation with o-xylenes, further reagent: tmen, multistep reaction; Product distribution;
参考文献
Leung, Wing-Por; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1801 - 1808
反应条件
n-butyllithium; pmdien in hexane
Ambient temperaturelithiation of p-xylene compounds, comparation with o-xylenes, further reagent: tmen, multistep reaction; Product distribution;
参考文献
Leung, Wing-Por; Raston, Colin L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1801 - 1808