反应条件
LDA in tetrahydrofuran (inert atmosphere); addn. of LDA in THF at -78°C to the Ge compd.in THF, stirring 5 h while warming up to -30°C, addn. of Me3GeCl in THF, warming to room temp., quenching with satd. aq. NH4Cl; phase sepn., washing (H2O), drying (CaCl2), concn., gas chromy.;
参考文献
Eckert-Maksic, Mirjana; Elbel, Susanne; Stohlmeier, Michael; Untiedt, Sven; De Meijere, Armin
Chemische Berichte, 1996 , vol. 129, # 2 p. 169 - 174