1-甲基-2-苯基吲哚-3-甲醛合成路线 (共 24 条)
反应条件
1: 2-phenylindole-3-carboxaldehyde With sodium hydride in N,N-dimethyl-formamide; mineral oil 0.166667 h; Inert atmosphere; 2: methyl iodide in N,N-dimethyl-formamide; mineral oil T=20°C; 1 h; Inert atmosphere;
参考文献
Thorley, Karl J.; Hales, Joel M.; Kim, Hyeongeu; Ohira, Shino; Bredas, Jean-Luc; Perry, Joseph W.; Anderson, Harry L.
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10370 - 10377
反应条件
oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride in N,N-dimethyl-formamide T=130°C; P=760.051 Torr; 24 h;
参考文献
Ding, Shengtao; Jiao, Ning
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12374 - 12377
反应条件
oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride in N,N-dimethyl-formamide T=130°C; P=760.051 Torr; 24 h;
参考文献
Ding, Shengtao; Jiao, Ning
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12374 - 12377
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in 1,2-dichloro-ethane T=87°C; 40 h; Inert atmosphere;
参考文献
Wu, Cui-Yan; Hu, Ming; Liu, Yu; Song, Ren-Jie; Lei, Yong; Tang, Bo-Xiao; Li, Rong-Jiang; Li, Jin-Heng
Chemical Communications, 2012 , vol. 48, # 26 p. 3197 - 3199
反应条件
oxygen; copper dichloride in water; dimethyl sulfoxide T=120°C; 4 h;
参考文献
Chen, Jianbin; Liu, Bin; Liu, Dongfang; Liu, Shan; Cheng, Jiang
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2438 - 2442
反应条件
oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride in N,N-dimethyl-formamide T=130°C; P=760.051 Torr; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 133, # 32 p. 12374 - 12377
反应条件
oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride in N,N-dimethyl-formamide T=130°C; P=760.051 Torr; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 133, # 32 p. 12374 - 12377
反应条件
oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride T=130°C; P=760.051 Torr; 29 h;
参考文献
Ding, Shengtao; Jiao, Ning
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12374 - 12377
反应条件
ammonium acetate; water T=150°C; 40 h; Inert atmosphereSealed tube;
参考文献
Fei, Haiyang; Yu, Jintao; Jiang, Yan; Guo, Huan; Cheng, Jiang
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 41 p. 7092 - 7095
反应条件
oxygen; iron(III) chloride in acetonitrile Oxidation; 1.5 h;
参考文献
Chemical Research in Toxicology, , vol. 11, # 10 p. 1184 - 1194