1-甲基-2-苯基吲哚-3-甲醛合成路线 （共 24 条）
反应条件
oxygen; iron(III) chloride in acetonitrile Oxidation; 1.5 h;
参考文献
Chemical Research in Toxicology, , vol. 11, # 10 p. 1184 - 1194
反应条件
1: POCl3 / 80 °C 2: 84 percent / KOBut / 2-methyl-propan-2-ol View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 3 p. 377 - 380
反应条件
oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride T=130°C; P=760.051 Torr; 24 h;
参考文献
Ding, Shengtao; Jiao, Ning
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12374 - 12377
反应条件
1: 32 percent / methanesulfonic acid / various solvent(s) / 24 h / 20 °C 2: 78 percent / FeCl3; O2 / acetonitrile / 1.5 h View Scheme
参考文献
Chemical Research in Toxicology, , vol. 11, # 10 p. 1184 - 1194
反应条件
1: N,N-dimethylaniline / 170 °C 2: POCl3 / 80 °C 3: 84 percent / KOBut / 2-methyl-propan-2-ol View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 3 p. 377 - 380
反应条件
1: N,N-dimethylaniline / 170 °C 2: POCl3 / 80 °C 3: 84 percent / KOBut / 2-methyl-propan-2-ol View Scheme
参考文献
Tetrahedron Letters, , vol. 46, # 3 p. 377 - 380
反应条件
trichlorophosphate T=35°C; Behandeln des erhaltenen Reaktionsgemisches mit Wasser;
参考文献
Journal of the Chemical Society, , p. 3388,3396
反应条件
1: formic acid / 4 h / Reflux 2: oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride / N,N-dimethyl-formamide / 24 h / 130 °C / 760.05 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 32 p. 12374 - 12377
反应条件
1: sodium tetrahydroborate; NiII chloride hexahydrate / methanol / 1 h 2: formic acid / 4 h / Reflux 3: oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride / N,N-dimethyl-formamide / 24 h / 130 °C / 760.05 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 32 p. 12374 - 12377
反应条件
1: sodium tetrahydroborate / ethanol / 18 h 2: oxygen; tetra-n-butylammonium acetate; palladium diacetate; potassium carbonate; copper(ll) bromide; iron(II) chloride / N,N-dimethyl-formamide / 24 h / 130 °C / 760.05 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 32 p. 12374 - 12377
