反应条件
1: 1.) NaH / 1.) THF, room temperature - 30 min, reflux - 15 min, 2.) THF, room temperature, 20 h
2: 100 percent / aq. NaOH / 24 h / Heating
3: ceric ammonium sulfate
4: NH3
View Scheme
参考文献
Roberts, David; Joule, John A.; Antonieta Bros; Alvarez, Mercedes
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 568 - 577
