(2R,3R)-2,3-环氧丁烷反式合成路线 (共 18 条)
反应条件
trilithium phosphate T=240 - 315°C;
参考文献
Farberov; Bondarenko; Obukhov; Stepanova; Srednev; Vasil'eva
Journal of applied chemistry of the USSR, 1984 , vol. 57, # 11 pt 2 p. 2385 - 2388
反应条件
ammonium chloride; zinc; cyanocobalamin in methanol 30 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Su, Heng; Walder, Lorenz; Zhang, Zhong-da; Scheffold, Rolf
Helvetica Chimica Acta, 1988 , vol. 71, p. 1073 - 1078
反应条件
orthophosphorus acid; acetic anhydride in 1,4-dioxane 12 h; Ambient temperature;
参考文献
Klosinski
Tetrahedron Letters, 1990 , vol. 31, # 14 p. 2025 - 2028
反应条件
magnesium bromide in N,N-dimethyl-formamide T=130°C; 4 h;
参考文献
Petroleum Chemistry, , vol. 43, # 3 p. 167 - 169
反应条件
diethyl ether; magnesium bromide; benzene
参考文献
Usines de Melle
Patent: US2167203 , 1937 ;
Full Text Show Details
Usines de Melle
Patent: FR815494 , 1936 ;
反应条件
in various solvent(s)
T=40°C; 0.5 h;
参考文献
Petrova, L. S.; Davidenkov, L. R.; Medved', S. S.
J. Appl. Chem. USSR (Engl. Transl.), 1980 , vol. 53, # 1 p. 199 - 203,174 - 178
反应条件
(i) Li, (ii) /BRN= 102413/, (iii) aq. Na2Cr2O7, H2SO4; Multistep reaction;
参考文献
Stang,P.J.; Dueber,T.E.
Journal of the American Chemical Society, 1977 , vol. 99, # 8 p. 2602 - 2610
反应条件
sodium ethanolate in ethanol
参考文献
Wamhoff, Heinrich; Thiemig, Heinz-Albrecht
Chemische Berichte, 1985 , vol. 118, # 11 p. 4473 - 4485