(9aS)-六氢-1H-吡咯并[2,1-d][1,2,5]三氮杂卓-1,5(2H)-二酮合成路线 (共 2 条)
反应条件
ammonia; sodium in tetrahydrofuran T=-60°C; 0.25 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 16 p. 2297 - 2311
反应条件
Multi-step reaction with 3 steps 1: NMM, iso-butyl chloroformate / tetrahydrofuran; dimethylformamide / -40 °C2: H2NNH2*H2O / ethanol / Heating3: ethanol / 1.5 h / Heating
参考文献
Lenman, Morag M.; Ingham, Scott L.; Gani, David Journal of the Chemical Society, Chemical Communications, 1996 , # 1 p. 85 - 88