1,4,7-三叔丁氧羰基-1,4,7,10-四氮杂环十二烷合成路线 (共 9 条)
反应条件
triethylamine in chloroform
参考文献
Liu, Kun; Meyerhoff, Mark E.
Journal of Materials Chemistry, 2012 , vol. 22, # 36 p. 18784 - 18787
反应条件
hydrogen; palladium on activated charcoal
参考文献
Kimura, Eiichi; Aoki, Shin; Koike, Tohru; Shiro, Motoo
Journal of the American Chemical Society, 1997 , vol. 119, # 13 p. 3068 - 3076
反应条件
in chloroform T=20°C;
参考文献
Tetrahedron Letters, , vol. 47, # 39 p. 6937 - 6940
反应条件
1: sulfuric acid / neat (no solvent) / 0.05 h / 100 °C / |Microwave irradiation 2: triethylamine / chloroform / 28 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Research on Chemical Intermediates, , vol. 38, # 8 p. 2085 - 2096
反应条件
1: 74 percent / sodium carbonate / acetonitrile / 48 h / Heating 2: 85 percent / 6 M HCl / 1 h / 80 °C View Scheme
参考文献
Brandes, Stephane
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 1 p. 65 - 73
参考文献
Kimura, Eiichi; Aoki, Shin; Koike, Tohru; Shiro, Motoo
Journal of the American Chemical Society, 1997 , vol. 119, # 13 p. 3068 - 3076
反应条件
1.1: Na2CO3 / acetonitrile / Heating 2.1: NaOH / methanol; H2O / 2 h 2.2: citric acid / H2O / pH 5 View Scheme
参考文献
Organic Letters, , vol. 4, # 23 p. 4155 - 4158
反应条件
potassium carbonate in acetonitrile
96 h; Heating;
参考文献
Krivickas, Sara J.; Tamanini, Emiliano; Todd, Matthew H.; Watkinson, Michael
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8280 - 8289
反应条件
potassium carbonate in acetonitrile
Heating;
参考文献
Krivickas, Sara J.; Tamanini, Emiliano; Todd, Matthew H.; Watkinson, Michael
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8280 - 8289