三丁基(2,3-二氢噻吩并[3,4-b]-[1,4]二恶英-5-基)锡烷合成路线 （共 4 条）
反应条件
1: 2,3-dihydro-thieno[3,4-b][1,4]dioxine With n-butyllithium in tetrahydrofuran; hexane T=-78 - 40°C; 1 h; Inert atmosphere; 2: tributyltin chloride in tetrahydrofuran; hexane T=-40°C; 12.1667 h; Inert atmosphere;
参考文献
NATIONAL INSTITUTE FOR MATERIALS SCIENCE; Saint Gobain Glass France; ASHRAFUL, Islam; HATA, Kawae; HAN, Liyuan
Patent: WO2013/8951 A1, 2013 ;
Location in patent: Page/Page column 34-35 ;
反应条件
in tetrahydrofuran; hexane
参考文献
The United States of America as represented by the Secretary of the Air Force
Patent: US6130339 A1, 2000 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride; n-butyllithium in tetrahydrofuran; hexane; N,N-dimethyl-formamide T=130°C; 15 h;
参考文献
Chen, Xiao-Yan; Yang, Xiaoping; Holliday, Bradley J.
Journal of the American Chemical Society, 2008 , vol. 130, # 5 p. 1546 - 1547
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Stille coupling; 24 h; Inert atmosphereReflux;
参考文献
Molecular Crystals and Liquid Crystals, , vol. 493, p. 82 - 92
