(S)-2-苯基-1-丙胺合成路线 (共 26 条)
反应条件
1: CB / diethyl ether / 12 h / 0 deg C to r. t. 2: H2 / Raney-Ni / methanol / 24 h / 20 - 40 °C / 2625.2 - 2850.2 Torr View Scheme
参考文献
Angewandte Chemie, , vol. 96, # 5 p. 368 - 369
反应条件
1: pyridine 2: NaN3 / dimethylsulfoxide / 20 h / 80 °C 3: LiAlH4 / diethyl ether View Scheme
参考文献
Chemische Berichte, , vol. 113, # 6 p. 2140 - 2153
反应条件
1: NaN3 / dimethylsulfoxide / 20 h / 80 °C 2: LiAlH4 / diethyl ether View Scheme
参考文献
Chemische Berichte, , vol. 113, # 6 p. 2140 - 2153
反应条件
1: With formamide Condensation; Leuckart reaction; 10 h; Heating; 2: With sodium hydroxide Hydrolysis; Leuckart reaction; 15 h; Heating; Title compound not separated from byproducts;
参考文献
European Journal of Medicinal Chemistry, , vol. 34, # 4 p. 293 - 300
反应条件
lithium aluminium tetrahydride Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 191 - 192
反应条件
lithium aluminium tetrahydride
参考文献
Angewandte Chemie, , vol. 103, # 8 p. 907 - 915
反应条件
1: 600 °C / flash pyrolysis 2: LiAlH4 View Scheme
参考文献
Angewandte Chemie, , vol. 103, # 8 p. 907 - 915
反应条件
immobilized Candida antarctica lipase B (EC 3.1.1.1.) T=30°C; P=5 Torr; 24 h; Enzymatic reaction; Product distribution;
参考文献
Tetrahedron Letters, , vol. 45, # 3 p. 523 - 525
反应条件
sodium nitrite in perchloric acid; water Product distributionMechanism;
参考文献
Kirmse, Wolfgang; Guenther, Bernd-Rainer; Loosen, Karin
Chemische Berichte, 1980 , vol. 113, # 6 p. 2140 - 2153
反应条件
anschliessendes Erwaermen auf 60grad;
参考文献
Levene; Marker
Journal of Biological Chemistry, 1933 , vol. 103, p. 373,376, 380