2,3-二氟-4-羟基苯甲酸合成路线 (共 8 条)
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=25°C; 2 h;
参考文献
Marzi, Elena; Gorecka, Joanna; Schlosser, Manfred
Synthesis, 2004 , # 10 p. 1609 - 1618
反应条件
1: K2CO3 2: butyllithium / -78 °C 3: H2 / Pd/C View Scheme
参考文献
Journal of Materials Chemistry, , vol. 17, # 8 p. 766 - 782
反应条件
1.1: BuLi; 2,2,6,6-teramethylpiperidine / tetrahydrofuran; hexane / 2 h / -75 °C 1.2: tetrahydrofuran; hexane 2.1: 3.87 g / TBAF / tetrahydrofuran / 2 h / 25 °C View Scheme
参考文献
Synthesis, , # 10 p. 1609 - 1618
反应条件
hydrogen; palladium on activated charcoal
参考文献
Journal of Materials Chemistry, , vol. 17, # 8 p. 766 - 782
反应条件
1: butyllithium / -78 °C 2: H2 / Pd/C View Scheme
参考文献
Journal of Materials Chemistry, , vol. 17, # 8 p. 766 - 782
反应条件
1: butyllithium / -78 °C 2: hydrogen peroxide 3: K2CO3 4: butyllithium / -78 °C 5: H2 / Pd/C View Scheme
参考文献
Journal of Materials Chemistry, , vol. 17, # 8 p. 766 - 782
反应条件
1: hydrogen peroxide 2: K2CO3 3: butyllithium / -78 °C 4: H2 / Pd/C View Scheme
参考文献
Journal of Materials Chemistry, , vol. 17, # 8 p. 766 - 782
反应条件
sodium hydroxide 7 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 121, # 1 p. 97 - 99