N-三甲基硅基苯甲醛亚胺合成路线 （共 59 条）
反应条件
n-butyllithium; benzaldehyde in hexane
参考文献
Rhone-Poulenc Rorer S.A.
Patent: US5726346 A1, 1998 ;
反应条件
n-butyllithium 1) 5 min, 2) 10 min, ice bath;
参考文献
Hart, David J.; Kanai, Ken-ichi; Thomas, Dudley G.; Yang, Teng-Kuei
Journal of Organic Chemistry, 1983 , vol. 48, # 3 p. 289 - 294
反应条件
chloro-trimethyl-silane
参考文献
Bayard, Philippe; Ghosez, Leon
Tetrahedron Letters, 1988 , vol. 29, # 47 p. 6115 - 6118
反应条件
1: LiHMDSA / heptane; hexane / 1 h / 0 °C 2: heptane / 0 - 20 °C View Scheme
参考文献
Bongini, Alessandro; Panunzio, Mauro; Bandini, Elisa; Campana, Eileen; Martelli, Giorgio; Spunta, Giuseppe
Tetrahedron Asymmetry, 2001 , vol. 12, # 3 p. 439 - 454
反应条件
lithium aluminium tetrahydride; ethyl acetate in diethyl ether 0 deg C, 1 hr. then room temp., 2 hrs.;
参考文献
Andreoli, P.; Cainelli, G.; Contento, M.; Giacomini, D.; Martelli, G.; Panunzio, M.
Tetrahedron Letters, 1986 , vol. 27, # 15 p. 1695 - 1698
反应条件
in n-heptane T=0 - 20°C;
参考文献
Bongini, Alessandro; Panunzio, Mauro; Bandini, Elisa; Campana, Eileen; Martelli, Giorgio; Spunta, Giuseppe
Tetrahedron Asymmetry, 2001 , vol. 12, # 3 p. 439 - 454
反应条件
lithium hexamethyldisilazane 1.) THF, 0 deg C, 30 min, 2.) THF, 30 min; Yield given. Multistep reaction;
参考文献
Ojima, Iwao; Habus, Ivan; Zhao, Mangzhu; Zucco, Martine; Park, Young Hoon; Sun, Chung Ming; Brigaud, Thierry
Tetrahedron, 1992 , vol. 48, # 34 p. 6985 - 7012
参考文献
Hoberg,H.; Goetz,V.
Journal of Organometallic Chemistry, 1976 , vol. 118, p. C3 - C5
反应条件
in tetrahydrofuran Condensation; Aza-Wittig reaction; 3 h; Heating;
参考文献
Hemming; Bevan; Loukou; Patel; Renaudeau
Synlett, 2000 , # 11 p. 1565 - 1568
反应条件
LiN(SiHMe2)t-Bu 1.) THF, n-hexane, -10 to 20 deg C, 4 h; 20 deg C, 10 h, 2.) THF, n-hexane, 40 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schneider, Jan; Popowski, Eckhard; Fuhrmann, Hans
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1998 , vol. 53, # 7 p. 663 - 672
