N-三甲基硅基苯甲醛亚胺合成路线 （共 59 条）
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schneider, Jan; Popowski, Eckhard; Fuhrmann, Hans
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1998 , vol. 53, # 7 p. 663 - 672
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schneider, Jan; Popowski, Eckhard; Fuhrmann, Hans
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1998 , vol. 53, # 7 p. 663 - 672
反应条件
multistep reaction different solvents and reaction conditions; Product distribution;
参考文献
Schneider, Jan; Popowski, Eckhard; Fuhrmann, Hans
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1998 , vol. 53, # 7 p. 663 - 672
反应条件
1.1: titanium(IV) isopropylate; cyclopentyl-magnesium chloride / tetrahydrofuran; diethyl ether / 1.5 h / -78 - -30 °C / Inert atmosphere 1.2: 0.17 h / -78 - 0 °C / Inert atmosphere 1.3: 0 - 20 °C / Inert atmosphere 2.1: silver nitrate / ethanol; water / 60 °C / Inert atmosphere View Scheme
参考文献
Chen, Ming Z.; Micalizio, Glenn C.
Journal of the American Chemical Society, 2012 , vol. 134, # 2 p. 1352 - 1356
反应条件
in tetrahydrofuran T=-70 - 0°C; 2 h;
参考文献
Hart, David J.; Kanai, Ken-ichi; Thomas, Dudley G.; Yang, Teng-Kuei
Journal of Organic Chemistry, 1983 , vol. 48, # 3 p. 289 - 294
反应条件
in tetrahydrofuran 18 h; Heating;
参考文献
Hart, David J.; Kanai, Ken-ichi; Thomas, Dudley G.; Yang, Teng-Kuei
Journal of Organic Chemistry, 1983 , vol. 48, # 3 p. 289 - 294
反应条件
1: tri-isobutyl aluminium; hydrogen / toluene / 24 h / 100 °C / 77525.2 Torr 2: water / ethyl acetate / |Inert atmosphere; |Glovebox; |Schlenk technique View Scheme
参考文献
Hatnean, Jillian A.; Thomson, Jordan W.; Chase, Preston A.; Stephan, Douglas W.
Chemical Communications, 2014 , vol. 50, # 3 p. 301 - 303
反应条件
in diethyl ether T=20°C; Addition; 0.5 h;
参考文献
Saidi, Mohammad R.; Javanshir, Shahrzad; Mojtahedi, Mohammad M.
Journal of Chemical Research - Part S, 1999 , # 5 p. 330 - 331
反应条件
in tetrahydrofuran 40 h; Heating;
参考文献
Hart, David J.; Kanai, Ken-ichi; Thomas, Dudley G.; Yang, Teng-Kuei
Journal of Organic Chemistry, 1983 , vol. 48, # 3 p. 289 - 294
反应条件
in chloroform T=55°C; 2 h;
参考文献
Wu, T. Robert; Chong, J. Michael
Organic Letters, 2006 , vol. 8, # 1 p. 15 - 18
