1,4-二硫杂螺[4.4]壬烷合成路线 (共 5 条)
反应条件
silica gel; bis(trimethylsilyl)sulphate in dichloromethane 1 h; Ambient temperature;
参考文献
Patney, Harish K.
Tetrahedron Letters, 1994 , vol. 35, # 31 p. 5717 - 5718
反应条件
di-n-butylbis(trifluoromethanesulfonyloxy)stannane in 1,2-dichloro-ethane T=35°C; 20 h;
参考文献
Sato, Tsuneo; Otera, Junzo; Nozaki, Hitosi
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4971 - 4978
反应条件
indium(III) chloride in 1,2-dichloro-ethane 0.2 h; Heating;
参考文献
Ranu, Brindaban C.; Das, Arijit; Samanta, Sampak
Synlett, 2002 , # 5 p. 727 - 730
反应条件
trimethylsilyl bromide; dimethyl sulfoxide in tetrachloromethane T=75 - 80°C; 24 h;
参考文献
Olah, George A.; Narang, Subbash C.; Mehrotra, Ashok K.
Synthesis, 1982 , # 11 p. 965 - 966
反应条件
oxygen; naphthalenyl-1-carbonitrile in water; acetonitrile
Irradiation;
参考文献
Pandey, Bipin; Bal, Smita Y.; Khire, Uday R.
Tetrahedron Letters, 1989 , vol. 30, # 30 p. 4007 - 4008