2-(4-氯苯基)乙基 异硫代氰酸酯合成路线 (共 3 条)
反应条件
1: 4-chlorophenethyl azide With hydrogen; Lindlar's catalyst in ethanol 2 h; 2: 1,1'-Thiocarbonyldi-2(1H)-pyridone in dichloromethane T=20°C; 16 h;
参考文献
Lee, Jeewoo; Lee, Jiyoun; Szabo, Tamas; Gonzalez, Adamar F.; Welter, Jacqueline D.; Blumberg, Peter M.
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 7 p. 1713 - 1720
反应条件
in N,N-dimethyl-formamide T=55°C; 1.5 h; Molecular sieve;
参考文献
European Journal of Medicinal Chemistry, , vol. 69, p. 244 - 261
参考文献
US2005/165004 A1, ;
Page/Page column 6-7 ;