3,5-双(叔丁基)苯甲醛合成路线 （共 43 条）
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane
T=20°C; 3 h;
2: With chloranil in dichloromethane
1 h; Heating;
参考文献
Richeter, Sebastien; Jeandon, Christophe; Kyritsakas, Nathalie; Ruppert, Romain; Callot, Henry J.
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9200 - 9208
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane
1.5 h;
2: With chloranil in dichloromethane
1.5 h;
参考文献
Richeter, Sebastien; Jeandon, Christophe; Kyritsakas, Nathalie; Ruppert, Romain; Callot, Henry J.
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9200 - 9208
反应条件
1: With methanesulfonic acid in dichloromethane
0.5 h;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
0.166667 h;
参考文献
Shaw, Janet L.; Garrison, Shana A.; Aleman, Elvin A.; Ziegler, Christopher J.; Modarelli, David A.
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7423 - 7427
反应条件
boron trifluoride diethyl etherate in dichloromethane
参考文献
Smeets, Stefan; Dehaen, Wim
Tetrahedron Letters, 1998 , vol. 39, # 52 p. 9841 - 9844
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane
Condensation;
2: With chloranil
Dehydrogenation;
参考文献
Motmans, Filip; Ceulemans, Erik; Smeets, Stefan; Dehaen, Wim
Tetrahedron Letters, 1999 , vol. 40, # 42 p. 7545 - 7548
反应条件
1: With trichloroacetic acid in dichloromethane
T=20°C; 17 h;
2: With chloranil in dichloromethane
3 h;
参考文献
Suga; Arimura; Ide; Nishioka; Sugihara; Murata; Tsuzuki
Journal of Chemical Research - Part S, 2000 , # 11 p. 512 - 514
反应条件
in propionic acid
16 h; Heating;
参考文献
Chardon-Noblat, Sylvie; Sauvage, Jean-Pierre; Mathis, Paul
Angewandte Chemie, 1989 , vol. 101, # 5 p. 631 - 632
反应条件
boron trifluoride diethyl etherate; 1,2,3-thiadiazole-4-carboxaldehyde in dichloromethane
参考文献
Smeets, Stefan; Dehaen, Wim
Tetrahedron Letters, 1998 , vol. 39, # 52 p. 9841 - 9844
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane
Condensation;
2: With chloranil
Dehydrogenation;
参考文献
Motmans, Filip; Ceulemans, Erik; Smeets, Stefan; Dehaen, Wim
Tetrahedron Letters, 1999 , vol. 40, # 42 p. 7545 - 7548
反应条件
oxygen; chloroacetic acid in xylene
4 h; Heating;
参考文献
Ishkov, Yu. V.; Zhilina, Z. I.; Grushevaya, Zh. V.; Voloshanovskii, I. S.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 11 p. 2101 - 2106
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 11 p. 2433 - 2440
