四(2-羟基乙基)原硅酸溶液合成路线 (共 3 条)
反应条件
sulfonic acid type-ion exchange resin
T=85°C; 4 h; DowEX 50W-X8; Product distribution / selectivity;
参考文献
SHISEIDO COMPANY, LTD.
Patent: EP1930337 A1, 2008 ;
Location in patent: Page/Page column 9 ;
反应条件
ethylene glycol
shaking of Si(OC2H5)4 and (CH2OH)2 at 50-60°C;;
参考文献
Knorr, L.; Weyland, H.
Patent: DE285285 , 1915 ;
C. II, 1915 , p. 373
Full Text Show Details
Synthetic Patents Co.
Patent: US1178731 , 1916 ;
反应条件
potassium fluoride
T=107°C; varying of molar ratios of reactants and catalyst, reaction temperature, CsF; Product distributionMechanism;
参考文献
Kopylov, V. M.; Shapatin, A. S.; Gracheva, O. D.; Tandura, S. N.; Prikhod'ko, P. L.
J. Gen. Chem. USSR (Engl. Transl.), 1987 , vol. 57, # 10 p. 2333 - 2336,2086 - 2088