2-(2-丙基)-1,3-苯并噻唑合成路线 （共 24 条）
反应条件
trifluoroacetic acid in dichloromethane
T=20°C; 43 h; Inert atmosphere;
参考文献
Zhu, Chen; Akiyama, Takahiko
Synlett, 2011 , # 9 art. no. Y03711ST, p. 1251 - 1254
反应条件
buta-1,3-diene; nickel dichloride in tetrahydrofuran
T=-78 - 50°C; P=760.051 Torr; Schlenk techniqueInert atmosphere;
参考文献
Ghaderi, Arash; Iwasaki, Takanori; Fukuoka, Asuka; Terao, Jun; Kambe, Nobuaki
Chemistry - A European Journal, 2013 , vol. 19, # 9 p. 2951 - 2955
反应条件
tert.-butylhydroperoxide; ferric acetate; trifluoroacetic acid in acetic acid
4 h; Heating;
参考文献
Fontana, Francesca; Minisci, Francesco; Barbosa, Maria Claudia Nogueira; Vismara, Elena
Acta Chemica Scandinavica, 1989 , vol. 43, # 10 p. 995 - 999
反应条件
T=200°C; 0.166667 h; Irradiationmicrowave;
参考文献
Kamila, Sukanta; Koh, Benjamin; Biehl, Edward R.
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 6 p. 1609 - 1612
反应条件
1: 93 percent / sodium ethoxide / ethanol / 1 h / Heating
2: 82 percent / 250 °C
View Scheme
参考文献
Landor, Stephen R.; Landor, Phyllis D.; Fomum, Z. Tanee; Mbafor, J. Tanyi; Mpango, George W. B.
Tetrahedron, 1984 , vol. 40, # 11 p. 2141 - 2149
反应条件
1: 79 percent / tetrahydrofuran / 2 h / 0 °C
2: 87 percent / NaH / toluene; dimethylformamide / 10.5 h / Heating
View Scheme
参考文献
Ares
Synthetic Communications, 1991 , vol. 21, # 5 p. 625 - 633
反应条件
1: n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature
2: n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature
View Scheme
参考文献
Florio, S.; Troisi, L.
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3721 - 3724
反应条件
n-butyllithium
1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Florio, S.; Troisi, L.
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3721 - 3724
反应条件
silica gel
0.0833333 h; microwave irradiation;
参考文献
Kodomari, Mitsuo; Tamaru, Yoshimi; Aoyama, Tadashi
Synthetic Communications, 2004 , vol. 34, # 16 p. 3029 - 3036
反应条件
zinc
1.) CHCl3, reflux, 0.5 h, 2.) reflux, 1 h; Yield given. Multistep reaction;
参考文献
Quast, Helmut; Ach, Manfred; Kindermann, Markus K.; Rademacher, Paul; Schindler, Michael
Chemische Berichte, 1993 , vol. 126, # 2 p. 503 - 516
