2-叔丁基-1,3-苯并噻唑合成路线 （共 41 条）
反应条件
in chlorobenzene
thermolysis;
参考文献
Hori, Mikio; Kataoka, Tadashi; Shimizu, Hiroshi; Ueda, Norihiro
Tetrahedron Letters, 1981 , vol. 22, # 32 p. 3071 - 3074
反应条件
sodium peroxodisulphate; sulfuric acid; silver nitrate in dichloromethane; water
2 h; Heating;
参考文献
Coppa, Fausta; Fontana, Francesca; Lazzarini, Edoardo; Minisci, Francesco; Pianese, Giuseppe; Zhao, Lihua
Chemistry Letters, 1992 , # 7 p. 1295 - 1298
反应条件
1: 52 percent / Na2CO3 / H2O; diethyl ether / 1.) cooling with ice, 10 min, 2.) to r.t.
2: 30 percent / dimethylformamide / cathodic reduction, Hg cathode
View Scheme
参考文献
Gade, Thomas; Streek, Michael; Voss, Juergen
Chemische Berichte, 1992 , vol. 125, # 1 p. 127 - 142
反应条件
tert.-butylhydroperoxide; sulfuric acid; iron(II) sulfate in acetic acid
参考文献
Caronna,T. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 1747 - 1750
反应条件
tert.-butyl lithium
1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Kuzmierkiewicz, Wojciech; Aurrecoechea, Jose M.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 844 - 849
反应条件
1: n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature
2: n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature
3: n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature
View Scheme
参考文献
Florio, S.; Troisi, L.
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3721 - 3724
反应条件
1: n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature
2: n-BuLi / 1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature
View Scheme
参考文献
Florio, S.; Troisi, L.
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3721 - 3724
反应条件
n-butyllithium
1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Florio, S.; Troisi, L.
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3721 - 3724
反应条件
(i) Me2NCH2CH2NMe2, Et2O, (ii) SCl2; Multistep reaction;
参考文献
Walborsky,H.M.; Ronman,P.
Journal of Organic Chemistry, 1978 , vol. 43, # 4 p. 731 - 734
反应条件
in N,N-dimethyl-formamide
cathodic reduction, Hg cathode;
参考文献
Gade, Thomas; Streek, Michael; Voss, Juergen
Chemische Berichte, 1992 , vol. 125, # 1 p. 127 - 142
