1-(对甲苯磺酰基)吡咯合成路线 （共 50 条）
反应条件
NaH in tetrahydrofuran; water
参考文献
Frederich, James H.; Harran, Patrick G.
Journal of the American Chemical Society, 2013 , vol. 135, # 10 p. 3788 - 3791
反应条件
phosphorus pentoxide in toluene T=110°C; 0.333333 h;
参考文献
Fang; Leysen; Ottenheijm
Synthetic Communications, 1995 , vol. 25, # 12 p. 1857 - 1861
反应条件
1: With Grubb's 2nd generation catalyst in dichloromethane Heating; 2: With trifluoroacetic acid in dichloromethane T=20°C;
参考文献
Donohoe, Timothy J.; Orr, Allan J.; Gosby, Katherine; Bingham, Matilda
European Journal of Organic Chemistry, 2005 , # 10 p. 1969 - 1971
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene T=110°C; 5 h; Inert atmosphere;
参考文献
Shin, Ye Ho; Maheswara, Muchchintala; Hwang, Joon Young; Kang, Eun Joo
European Journal of Organic Chemistry, 2014 , vol. 2014, # 11 p. 2305 - 2311
反应条件
n-butyllithium; dimethyl-(4-nitro-buta-1,3-dienyl)-amine in tetrahydrofuran; pentane T=-78 - 20°C; Dehalogenation;
参考文献
Koike, Takeshi; Shinohara, Yoshifumi; Nishimura, Takeshi; Hagiwara, Masanori; Tobinaga, Seisho; Takeuchi, Naoki
Heterocycles, 2000 , vol. 53, # 6 p. 1351 - 1359
反应条件
copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide T=240°C; 2 h; Microwave irradiationInert atmosphere;
参考文献
Organic Letters, , vol. 12, # 21 p. 4872 - 4875
反应条件
1: With triphenoxyborane in toluene 0.0833333 h; Inert atmosphere; 2: With (SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in toluene 0.5 h; Inert atmosphereReflux;
参考文献
Shafi, Syed; Kedziorek, Mariusz; Grela, Karol
Synlett, 2011 , # 1 art. no. G30810ST, p. 124 - 128
反应条件
1: With triphenoxyborane in toluene 0.0833333 h; Inert atmosphere; 2: With (SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in toluene 0.5 h; Inert atmosphereReflux;
参考文献
Shafi, Syed; Kedziorek, Mariusz; Grela, Karol
Synlett, 2011 , # 1 art. no. G30810ST, p. 124 - 128
反应条件
1.1: 63 percent / dppp; Et3N; K2CO3 / Pd(OAc)2 / acetonitrile / Heating 2.1: Pcy3Cl2Ru=CHPh(diMesIm) / CH2Cl2 / Heating 2.2: 78 percent / TFA / CH2Cl2 / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 10 p. 1969 - 1971
反应条件
1: copper(I) bromide; N,N-dicyclohexylamine / 1,4-dioxane / 13 h / 110 °C 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 5 h / 110 °C / |Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 11 p. 2305 - 2311
