1-(对甲苯磺酰基)吡咯合成路线 （共 50 条）
反应条件
triethylamine; phosphorous acid trimethyl ester in methanol T=25°C; other substituted tosyl derivatives of thiazine oxide; Mechanism;
参考文献
Harrington; Sanchez
Synthetic Communications, 1994 , vol. 24, # 2 p. 175 - 180
反应条件
1: With triphenoxyborane in toluene 0.0833333 h; Inert atmosphere; 2: With (SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in toluene 0.5 h; Inert atmosphereReflux;
参考文献
Shafi, Syed; Kedziorek, Mariusz; Grela, Karol
Synlett, 2011 , # 1 art. no. G30810ST, p. 124 - 128
反应条件
toluene-4-sulfonic acid in dichloromethane T=25°C; 0.166667 h;
参考文献
Synlett, , # 1 art. no. G30810ST, p. 124 - 128
反应条件
1: RuCl2(tricyclohexylphosphine)2(benzylidene) / benzene / 0.5 h / 20 °C / Inert atmosphere 2: tert.-butylhydroperoxide / decane; benzene / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 26 p. 5119 - 5130
反应条件
1: potassium carbonate / acetonitrile / 12 h / 60 °C / Inert atmosphere 2: RuCl2(tricyclohexylphosphine)2(benzylidene) / benzene / 0.5 h / 20 °C / Inert atmosphere 3: tert.-butylhydroperoxide / decane; benzene / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 26 p. 5119 - 5130
反应条件
1: copper(I) bromide; N,N-dicyclohexylamine / 1,4-dioxane / 3 h / 180 °C / |Microwave irradiation 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 5 h / 110 °C / |Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 11 p. 2305 - 2311
反应条件
in various solvent(s) T=130°C; 0.5 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 23, # 19 p. 2051 - 2052
反应条件
1: 77 percent / K / tetrahydrofuran / 12 h / 20 °C View Scheme
参考文献
Australian Journal of Chemistry, , vol. 57, # 3 p. 227 - 232
参考文献
Australian Journal of Chemistry, , vol. 57, # 3 p. 227 - 232
反应条件
1: 97 percent / AlCl3 2: 97 percent / tetrahydrofuran / 0.25 h / -20 °C 3: 82 percent / 6percent H2SO4 / propan-2-ol / 0.5 h / Heating View Scheme
参考文献
Muratake, Hideaki; Natsume, Mitsutaka
Heterocycles, 1990 , vol. 31, # 4 p. 683 - 690
