1-(对甲苯磺酰基)吡咯合成路线 （共 50 条）
反应条件
aluminium trichloride
参考文献
Heterocycles, , vol. 31, # 4 p. 683 - 690
反应条件
ethylaluminum dichloride in 1,2-dichloro-ethane T=0°C; Friedel-Crafts reaction; 2 h;
参考文献
Huffman, John W.; Smith, Valerie J.; Padgett, Lea W.
Tetrahedron, 2008 , vol. 64, # 9 p. 2104 - 2112
反应条件
aluminium trichloride in dichloromethane 0.166667 h;
参考文献
Chen, Qingqi; Wang, Tianyu; Zhang, Yi; Wang, Qiuan; Ma, Jinshi
Synthetic Communications, 2002 , vol. 32, # 7 p. 1041 - 1049
反应条件
1.1: dichloromethane; trifluoroacetic anhydride / 20 °C 2.1: sodium tetrahydroborate / ethanol; dichloromethane / 0 - 20 °C 3.1: sodium cyanoborohydride / dichloromethane; acetic acid / 0 - 20 °C 4.1: dichloromethane; trifluoroacetic anhydride / 20 °C 5.1: sodium cyanoborohydride / dichloromethane; trifluoroacetic acid / 0 - 20 °C 5.2: 3.5 h / 2068.65 Torr View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 10 p. 3948 - 3953
反应条件
1: chloroacetyl chloride With AlCl3, aluminium chloride in dichloromethane T=20°C; 0.166667 h; 2: 1-tosyl-1H-pyrrole in dichloromethane T=20°C; 2 h;
参考文献
Serra Moreno, Judith; Agas, Dimitrios; Sabbieti, Maria Giovanna; Di Magno, Matteo; Migliorini, Antonella; Loreto, M. Antonietta
European Journal of Medicinal Chemistry, 2012 , vol. 57, p. 391 - 397
反应条件
sodium hydroxide; tin(IV) chloride Multistep reaction;
参考文献
Masuda, Hideyuki; Tanaka, Susum,; Kaeriyama, Kyoji
Journal of the Chemical Society, Chemical Communications, 1989 , # 11 p. 725 - 726
反应条件
Thiocyanogen chloride in acetic acid
0.5 h; Ambient temperature;
参考文献
Kakushima, Masatoshi; Frenette, Richard
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2025 - 2027
反应条件
aluminium trichloride; (SCN)2 in dichloromethane
参考文献
Kakushima, Masatoshi; Frenette, Richard
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2025 - 2027
反应条件
in acetic acid
0.25 h; Ambient temperature;
参考文献
Berlin, Anna; Pagani, Giorgio A.; Schiavon, Gilberto; Zotti, Gianni
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 5 p. 699 - 704
反应条件
1: 69 percent / ClSCN / acetic acid / 0.5 h / Ambient temperature
2: 1N NaOH / methanol / 2.5 h / Ambient temperature
View Scheme
参考文献
Kakushima, Masatoshi; Frenette, Richard
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2025 - 2027
