2,3,4,5,6-五氟溴化苄合成路线 （共 48 条）
反应条件
sulfuric acid; hydrogen bromide
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
bromine in tetrachloromethane
参考文献
Journal of Organic Chemistry, , vol. 34, # 3 p. 534 - 538
反应条件
N-bromosuccinmide T=36°C; 18 h; Irradiationneat (no solvent);
参考文献
Helvetica Chimica Acta, , vol. 92, # 3 p. 555 - 566
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-70 - 20°C; 19 h; MechanismProduct distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2023 - 2026
反应条件
1: (i) Mg, (ii) /BRN= 636496/ 2: LiAlH4 3: aq. HBr, H2SO4 View Scheme
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
1: LiAlH4 2: aq. HBr, H2SO4 View Scheme
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
1: (i) Mg, (ii) /BRN= 906769/ 2: LiAlH4 3: aq. HBr, H2SO4 View Scheme
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
1: aq. K2CO3 / Heating 2: aq. HBr, H2SO4 View Scheme
参考文献
Journal of the Chemical Society, , p. 808 - 817
反应条件
N,N,N',N'-tetramethyl-para-phenylenediamine; oxygen in acetonitrile 15 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Julliard, M.; Chanon, M.
Bulletin de la Societe Chimique de France, 1992 , # 3 p. 242 - 246
反应条件
1: 64 percent / LDA / tetrahydrofuran; hexane / from -60 degC to room temp. 2: 1.) trifluoroacetic acid; 2.) DOWEX 50 Wx 8 cation exchange resin / 1.) CH2Cl2, overnight; 2.) AcOH, 0.75 N HCl, 100 degC, 18 h View Scheme
参考文献
Fitzi, Robert; Seebach, Dieter
Tetrahedron, 1988 , vol. 44, # 17 p. 5277 - 5292
