2,3,4,5,6-五氟溴化苄合成路线 (共 48 条)
反应条件
18-crown-6 ether; potassium carbonate in acetone T=20°C; 96 h; Inert atmosphere;
参考文献
Quast, Matthew J.; Mueller, Anja
Journal of Polymer Science, Part A: Polymer Chemistry, 2014 , vol. 52, # 7 p. 985 - 994
反应条件
18-crown-6 ether; potassium carbonate in acetone T=40 - 60°C; Esterification; 3 h;
参考文献
Chien, Chao-Jung; Charles, M. Judith; Sexton, Kenneth G.; Jeffries, Harvey E.
Environmental Science and Technology, 1998 , vol. 32, # 2 p. 299 - 309
参考文献
Lacher, Sebastian; Matsuo, Yutaka; Nakamura, Eiichi
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 16997 - 17004
反应条件
1: aq. ethanol 2: aq. H2SO4, AcOH View Scheme
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
(i) Mg, I2, (ii) /BRN= 1900390/; Multistep reaction;
参考文献
Birchall,J.M.; Haszeldine,R.N.
Journal of the Chemical Society, 1961 , p. 3719 - 3727
反应条件
1: 97 percent / K2CO3 / acetone 2: AlCl3 View Scheme
参考文献
Xu, Linxiao; Giese, Roger W.
Tetrahedron Letters, 1993 , vol. 34, # 24 p. 3829 - 3832
反应条件
N,N,N',N'-tetramethyl-para-phenylenediamine; oxygen in acetonitrile 15 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Julliard, M.; Chanon, M.
Bulletin de la Societe Chimique de France, 1992 , # 3 p. 242 - 246
反应条件
2,2'-azo-bisisobutyronitrile; poly(phenylsilane) in benzene-d6 T=82 - 85°C; 3 h; sealed;
参考文献
Journal of Organometallic Chemistry, , vol. 545-546, p. 475 - 481
反应条件
T=727 - 800°C; ΔE(excit.); KineticsThermodynamic dataProduct distribution;
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 1906 - 1908
反应条件
1: aq. ethanol 2: aq. H2SO4, AcOH 3: FSO3H 4: LiAlH4 View Scheme
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817