N-苄氧羰基-L-亮氨酰-L-丙氨酸苯酯合成路线 (共 4 条)
反应条件
4-(N,N-dimethlyamino)pyridine; triphenylphosphine; 2aλ3-ioda-2,3-dioxa-cyclopenta[cd]indene-1,4-dione in chloroform T=60°C; 6 h;
参考文献
Tian, Jun; Gao, Wen-Chao; Zhou, Dong-Mei; Zhang, Chi
Organic Letters, 2012 , vol. 14, # 12 p. 3020 - 3023
反应条件
benzotriazol-1-ol; dicyclohexyl-carbodiimide
参考文献
Akazome, Motohiro; Hirabayashi, Atsushi; Takaoka, Kousuke; Nomura, Satoru; Ogura, Katsuyuki
Tetrahedron, 2005 , vol. 61, # 5 p. 1107 - 1113
反应条件
4-methyl-morpholine; chloroformic acid ethyl ester 1.) THF, -15 deg C, 5 min, 2.) CH2Cl2, -15 deg C, 4 h; room temperature, overnight; Yield given. Multistep reaction;
参考文献
Nakata; Takahashi; Nakatani; Kuramitsu; Tamura; Okai
Bioscience, biotechnology, and biochemistry, 1995 , vol. 59, # 4 p. 689 - 693
反应条件
palladium on activated charcoal; hydrogen in methanol 24 h; Ambient temperature;
参考文献
Nakata; Takahashi; Nakatani; Kuramitsu; Tamura; Okai
Bioscience, biotechnology, and biochemistry, 1995 , vol. 59, # 4 p. 689 - 693