3,5-二(3,5-二甲氧基苄氧基)苄醇合成路线 （共 4 条）
反应条件
dibenzo-18-crown-6; potassium carbonate in acetone 36 h; Inert atmosphereReflux;
参考文献
Fujimoto, Yuhei; Ubukata, Takashi; Yokoyama, Yasushi
Chemical Communications, 2008 , # 44 p. 5755 - 5757
反应条件
1: 61 percent / CBr4, Ph3P / tetrahydrofuran / 1 h 2: 1.) K2CO3, 18-crown-6-ether / 1.) acetone, reflux, 0.5 h, 2.) acetone, reflux, 42 h View Scheme
参考文献
Stewart, Gina M.; Fox, Marye Anne
Journal of the American Chemical Society, 1996 , vol. 118, # 18 p. 4354 - 4360
反应条件
18-crown-6 ether; potassium carbonate 1.) acetone, reflux, 0.5 h, 2.) acetone, reflux, 42 h; Yield given. Multistep reaction;
参考文献
Stewart, Gina M.; Fox, Marye Anne
Journal of the American Chemical Society, 1996 , vol. 118, # 18 p. 4354 - 4360
反应条件
carbon tetrabromide; triphenylphosphine Inert atmosphereSchlenk technique;
参考文献
Liu, Guoxing; Li, Ziyong; Wu, Di; Xue, Wen; Li, Tingting; Liu, Sheng Hua; Yin, Jun
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 643 - 652
