1-(2,3-二甲基苯基)-1-(1-三苯甲游基-1H-咪唑-5-基)乙醇合成路线 （共 7 条）
反应条件
triethylsilane; hydrogen; trifluoroacetic acid; palladium on activated charcoal 1.) r.t., CH2Cl2, 2.) r.t., 1 bar, 2 h, H2O; Yield given. Multistep reaction;
参考文献
Cordi, Alex A.; Persigand, Thierry; Lecouve, Jean-Pierre
Synthetic Communications, 1996 , vol. 26, # 8 p. 1585 - 1593
反应条件
triethylsilane; hydrogen; trifluoroacetic acid; palladium on activated charcoal 1.) r.t., CH2Cl2, 2.) r.t., 1 bar, 2 h, H2O; Yield given. Multistep reaction;
参考文献
Cordi, Alex A.; Persigand, Thierry; Lecouve, Jean-Pierre
Synthetic Communications, 1996 , vol. 26, # 8 p. 1585 - 1593
反应条件
in tetrahydrofuran
T=0 - 25°C; 3.5 h;
参考文献
"Joint Stock Company Grindeks"
Patent: EP1918282 A1, 2008 ;
Location in patent: Page/Page column 6 ;
反应条件
in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Cordi, Alex A.; Persigand, Thierry; Lecouve, Jean-Pierre
Synthetic Communications, 1996 , vol. 26, # 8 p. 1585 - 1593
反应条件
1: 1.) magnesium, iodine / 1.) THF, reflux, 1 h, 2.) r.t., THF, 1.5 h
2: 90 percent / MnO2 / dioxane / 5 h / Heating
3: 95 percent / tetrahydrofuran / 2 h / Ambient temperature
View Scheme
参考文献
Cordi, Alex A.; Persigand, Thierry; Lecouve, Jean-Pierre
Synthetic Communications, 1996 , vol. 26, # 8 p. 1585 - 1593
反应条件
1: 90 percent / MnO2 / dioxane / 5 h / Heating
2: 95 percent / tetrahydrofuran / 2 h / Ambient temperature
View Scheme
参考文献
Cordi, Alex A.; Persigand, Thierry; Lecouve, Jean-Pierre
Synthetic Communications, 1996 , vol. 26, # 8 p. 1585 - 1593
反应条件
1: 1.) magnesium, iodine / 1.) THF, reflux, 1 h, 2.) r.t., THF, 1.5 h
2: 90 percent / MnO2 / dioxane / 5 h / Heating
3: 95 percent / tetrahydrofuran / 2 h / Ambient temperature
View Scheme
参考文献
Cordi, Alex A.; Persigand, Thierry; Lecouve, Jean-Pierre
Synthetic Communications, 1996 , vol. 26, # 8 p. 1585 - 1593
