反应条件
in tetrahydrofuran all manipulations under dry N2; adding 7,7-dichlorobicyclo(4.1.0)heptane to suspn. of Na2Fe(CO)4 (vigorous stirring, -40°C), stirring (-40°C, 3 h); removing solvent (vacuum), extg. (petroleum ether, 40 - 60°C), filtering (kieselguhr), removing solvent, chromy. (silica gel, petroleum ether, 40 - 60°C), eluting 2 bands, first beeing desired complex, second Fe3(CO)12;
参考文献
Alam, S. S.; Hashem, M. A.; Ullah, S. S.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1988 , vol. 27, # 12 p. 1047 - 1049
