反应条件
in tetrahydrofuran Addn. of precooled THF (-76°C) to a mixt. of Pt- and Fe-complex, stirring to reach room temp. (1 h), stirring (room temp., overnight).; Evapn. to dryness, extg. (toluene), filtn., column chromy. (silica gel, CH2Cl2-hexane), 1. band Fe3(CO)12, red band of Fe2Pt(CO)8-complex, orange band of FePt2(CO)6-complex, brownisch band of Fe2Pt(CO)6-complex and orange band of FePt2(CO)4-complex.;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , # 12 p. 3801 - 3814