反应条件
in benzene
byproducts: 1,4-di(trimethylsilyl)-2,3,6,7-tetrathiacyclooctan, 1-methyl-3-trimethylsilyl-2,5-dithiacyclopentane; mixt. of educts in benzene stirred at 55°C for 8 h; evapd. in vac., extd. with pentane, evapd., chromd. (SiO2, hexane);
参考文献
Chernyshev, E.A.; Kuz'Min, O.V.; Lebedev, A.V.; Gusev, A.I.; Kirillova, N.I.; et. al.
Journal of Organometallic Chemistry, 1983 , vol. 252, # 2 p. 133 - 142
