反应条件
in benzene N2-atmosphere; slight excess of Si-compd., stirring (21°C, 24 h); evapn. (vac., cooling to just above freezing), dissoln. in hexane, standing at -30°C for several d, filtration off of Fe3(CO)12 (-30°C), evapn. of filtrate (low temp., vac.), distn. (0.001 Torr, probe at 0°C); elem. anal.;
参考文献
Cundy,C.S. et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 910 - 914
