反应条件
in methanol; hexane suspn. of Fe2(CO)9 and bicyclooctene in hexane/MeOH is stirred at room temp. for 14 h under Ar flux, then at 45°C for 24 h; evapn., taking up in hexane, filtn., addn. of acid alumina to decomposeFe3(CO)12, filtn., evapn., chromy. (silica gel, petroleum ether), recrystn. (hexane, -25°C);
参考文献
Helvetica Chimica Acta, , vol. 68, p. 126 - 134
