反应条件
in benzene N2-atmosphere; stirring of Fe-complex with silane (isomer mixt., Z:E=4:1) at 21°C for 40 h, evapn. (vac.), addn. of further Fe2(CO)9 and C6H6, standing for 40 h; evapn. (vac., cooling to just above freezing), dissoln. in hexane, standing at -30°C for several d, filtration off of Fe3(CO)12 (-30°C), evapn., distn. (0.001 Torr, probe at 0°C); isomer mixt. (4:1) not sepd.; elem. anal.;
参考文献
Cundy,C.S. et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 910 - 914
