反应条件
1: 1.) NaBr, ethyl bromide, (COCl)2 / 1.) DMF, MeCN, -18 deg C, 40 min, 2.) MeCN, -18 deg C, 45 min, 3.) pyridine, -18 deg C, 0.5 h; -18 deg C to room temperature, 20 h 2: 1.) t-BuOK, 2.) TFA / 1.) DMSO, 30 min, 2.) CH2Cl2, room temperature, 40 min View Scheme
参考文献
Henschke, Julian P.; Rickards, Rodney W.
Journal of Labelled Compounds and Radiopharmaceuticals, 1998 , vol. 41, # 3 p. 211 - 220
