2-溴-5-(1,3-恶唑-2-基)苯甲醛合成路线 （共 3 条）
反应条件
N,N,N-triethylamine N-oxide in dimethyl sulfoxide T=55°C; Oxidation; 6 h;
参考文献
Murugesan; Gu; Stein; Spergel; Mathur; Leith; Liu; Zhang; Bird; Waldron; Marino; Morrison; Webb; Moreland; Barrish
Journal of Medicinal Chemistry, 2000 , vol. 43, # 16 p. 3111 - 3117
反应条件
1: N-bromosuccinimide; benzoyl peroxide / CCl4 / 8 h / Heating; iluminating the solution with a sun lamp 2: triethylamine N-oxide / dimethylsulfoxide / 6 h / 55 °C View Scheme
参考文献
Murugesan; Gu; Stein; Spergel; Mathur; Leith; Liu; Zhang; Bird; Waldron; Marino; Morrison; Webb; Moreland; Barrish
Journal of Medicinal Chemistry, 2000 , vol. 43, # 16 p. 3111 - 3117
反应条件
1: 50 percent / polyphosphoric acid / 3 h / 170 °C 2: N-bromosuccinimide; benzoyl peroxide / CCl4 / 8 h / Heating; iluminating the solution with a sun lamp 3: triethylamine N-oxide / dimethylsulfoxide / 6 h / 55 °C View Scheme
参考文献
Murugesan; Gu; Stein; Spergel; Mathur; Leith; Liu; Zhang; Bird; Waldron; Marino; Morrison; Webb; Moreland; Barrish
Journal of Medicinal Chemistry, 2000 , vol. 43, # 16 p. 3111 - 3117
